Analysis of by-Products During Carbon Nanomaterial Synthesis

Tatsiana Henarava, Physical-Chemical Hydrodynamics Lab, A.V. Luikov Heat and Mass Transfer Institute of the National Academy of Sciences of Belarus, Minsk, Belarus (tatiana-susliako@mail.ru)
Siarhei Zhdanok, Academition Of The National Academy Of Sciences Of Belarus, National Academy Of Sciences Of Belarus, Minsk, Belarus
Oleg Penyazkov, Department Of Physics And Chemistry Of Non-equilibrium Media, A.v. Luikov Heat And Mass Transfer Institute Of The National Academy Of Sciences Of Belarus, Minsk, Belarus
Grushevskiy Vladimir, Heat and mass transfer institute of A.V. Luikov of the National Academy of Sciences of Belarus , Physical-Chemical Hydrodynamics Lab, Minsk, Belarus
Leschev Sergey, Belarussian State University ,Analytical Chemistry Department, Minsk, Belarus

Detailed analysis of all products during pyrolysis process for the carbon nanomaterial production is needed to clarify the nature of the substances formed, to understand the pyrolytic processes and to control the technological characteristics of the catalyst. Experimental studies were carried out at the temperature of 650-800 ° C. The carbon nanomaterial was obtained by catalytic pyrolysis of propane-butane mixture. The chemical composition of the samples was investigated by gas chromatography coupled with mass spectrometry (GC-MS).

By GC-MS it was found that catalytic pyrolysis is resulted to forming of carbon nanomaterial, gases (hydrogen, methane, carbon monoxide and other) and by-products. By-products consist of polycyclic aromatic hydrocarbons such as naphthalene, 2-methyl-naphthalene, biphenyl, biphenylene, acenaphthene, fluorene and anthracene.


Analysis of by-Products During Carbon Nanomaterial Synthesis Tatsiana Henarava, Physical-Chemical Hydrodynamics Lab, A.V. Luikov Heat and Mass Transfer Institute of the National Academy of Sciences of Belarus, Minsk, Belarus (tatiana-susliako@mail.ru) Siarhei Zhdanok, Academition Of The National Academy Of Sciences Of Belarus, National Academy Of Sciences Of Belarus, Minsk, Belarus Oleg Penyazkov, Department Of Physics And Chemistry Of Non-equilibrium Media, A.v. Luikov Heat And Mass Transfer Institute Of The National Academy Of Sciences Of Belarus, Minsk, Belarus Grushevskiy Vladimir, Heat and mass transfer institute of A.V. Luikov of the National Academy of Sciences of Belarus , Physical-Chemical Hydrodynamics Lab, Minsk, Belarus Leschev Sergey, Belarussian State University ,Analytical Chemistry Department, Minsk, Belarus Detailed analysis of all products during pyrolysis process for the carbon nanomaterial production is needed to clarify the nature of the substances formed, to understand the pyrolytic processes and to control the technological characteristics of the catalyst. Experimental studies were carried out at the temperature of 650-800 ° C. The carbon nanomaterial was obtained by catalytic pyrolysis of propane-butane mixture. The chemical composition of the samples was investigated by gas chromatography coupled with mass spectrometry (GC-MS). By GC-MS it was found that catalytic pyrolysis is resulted to forming of carbon nanomaterial, gases (hydrogen, methane, carbon monoxide and other) and by-products. By-products consist of polycyclic aromatic hydrocarbons such as naphthalene, 2-methyl-naphthalene, biphenyl, biphenylene, acenaphthene, fluorene and anthracene.

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